Isopropylamine → HCID 178426032, compound

Participants

Reaction Steps

In 10 ml of THF was dissolved 400 mg of N-[4-(heptafluoro-2-propyl)-2-methylphenyl]pyridine-2,3-dicarboximide-1-oxide, followed by adding thereto 200 mg of isopropylamine, and the resulting mixture was stirred at room temperature for 5 hours. After completion of the reaction, the solvent was distilled off under reduced pressure and the resulting residue was purified by a silica gel column chromatography using ethyl acetate/n-hexane as an eluent, to obtain 290 mg of the desired compound as white crystals.

Provenance & Evidence