HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20732811, compound → HCID 14863951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20732811 | HCID 20732811 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14863951 | HCID 14863951 | — |
Reaction Steps
A solution of acetal 15 (5.8 9, 0.02 mol) in EtOH (50 mL) was allowed to stir for 16 hours at room temperature over Raney nickel (0.2 g), in order to remove the trace amounts of sulphur impurities prior to hydrogenation. Excess nickel was removed by filtration through Celite.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06747144B1 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-5ffbb9d8496a4c7691dc131f96ab5b1a |
| Source note | uspto-grants-2004_06 |