HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 87998042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 87998041 | HCID 87998041 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 87998042 | HCID 87998042 | 122.2% |
Reaction Steps
In an amount of 15.0 g (19.2 mmol) of 1,5-di(3,3,4,4,5,5,6,6,6-nonafluorohexyl) glutamate p-toluenesulfonic acid salt and ethyl acetate were added with a saturated aqueous sodium hydrogencarbonate solution to wash the organic phase. Then, the organic layer was collected, and the organic solvent was evaporated under reduced pressure to obtain 15.0 g (yield: 74%) of the target compound as a yellow oily compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06747169B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-b837a43730fc4aafbf5bc47ec721548a |
| Source note | uspto-grants-2004_06 |