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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 352717Generated: October 31, 2026

Sodium Bicarbonate → HCID 87998042, compound

https://huagongshe.com/reaction/352717

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 87998041HCID 87998041—
SolventEthyl AcetateHCID 8857—
ProductHCID 87998042HCID 87998042122.2%

Reaction Steps

In an amount of 15.0 g (19.2 mmol) of 1,5-di(3,3,4,4,5,5,6,6,6-nonafluorohexyl) glutamate p-toluenesulfonic acid salt and ethyl acetate were added with a saturated aqueous sodium hydrogencarbonate solution to wash the organic phase. Then, the organic layer was collected, and the organic solvent was evaporated under reduced pressure to obtain 15.0 g (yield: 74%) of the target compound as a yellow oily compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06747169B2
Source datasetuspto-grants-2004_06
ORD IDord-b837a43730fc4aafbf5bc47ec721548a
Source noteuspto-grants-2004_06