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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 352981Generated: October 31, 2026

Trifluoroacetic acid → HCID 22710032, compound

https://huagongshe.com/reaction/352981

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 22709927HCID 22709927—
SolventDichloromethaneHCID 6344—
ProductHCID 22710032HCID 22710032—

Reaction Steps

To a solution of 1-[[6-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrooxazolo[5,4-c]pyridin-2-yl]carbonyl]-4-[(5-chloroindol-2-yl)sulfonyl]-2-ethylpiperazine (320 mg) in methylene chloride (5.0 ml) was added trifluoroacetic acid (5.0 ml) at room temperature, followed by stirring for 10 minutes. The reaction mixture was concentrated under reduced pressure, whereby the title compound (423 mg) was obtained as a pale brown solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06747023B1
Source datasetuspto-grants-2004_06
ORD IDord-ac0b885553ec446cbecf80d013ed9346
Source noteuspto-grants-2004_06