HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → Propionic acid, 3-(pyrrolidin-1-yl)-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Product | Propionic acid, 3-(pyrrolidin-1-yl)-, methyl ester | HCID 89167 | 95% |
Reaction Steps
Pyrrolidine, 71.1 g, was added to 86.1 g of methyl acrylate at 20° C. and reacted for 24 hours. Purification by vacuum distillation yielded 149 g of methyl 3-(1-pyrrolidinyl)propionate, designated [B-17] (boiling point: 74° C./800 Pa, yield: 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06749988B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-5b6a9a63597543de8c3263fa00753206 |
| Source note | uspto-grants-2004_06 |