Dimethylamine → HCID 178486089, compound

HRID 353055Notes

Reaction equation

HRID 353055 reaction equation
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[CH3:12][NH:13][CH3:14]>ClCCl>[CH3:11][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:12][N:13]([CH3:14])[SH:7](=[O:9])=[O:8]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 73974-Toluenesulfonyl chloride

Product 1

HCID 178486089HCID 178486089, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

To a stirring solution comprised of para-toluenesulfonyl chloride in dichloromethane at 0° C. is introduced excess gaseous dimethylamine. The precipitate is removed by filtration and the filtrate is concentrated in vacuo to obtain the product.

Workup

  1. customThe precipitate is removed by filtration
  2. concentrationthe filtrate is concentrated in vacuo
  3. customto obtain the product

Sources & evidence

ORD record
ord-aeb428a2a620458287160e625e1423d5
Source dataset
uspto-grants-2004_06
Patent number
US06750217B2

Reaction notes

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