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HRID353055

反应详情

EQUATION

反应方程式

HRID 353055 的结构方程式

REACTANTS

反应物

2
结构：CNC
HCID674

Dimethylamine

C2H7N

结构：Cc1ccc(S(=O)(=O)Cl)cc1
HCID7397

p-Toluenesulfonyl chloride

C7H7ClO2S

PRODUCTS

生成物

1
结构：CN(C)[SH](=O)=O.Cc1ccccc1
HCID178486089

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

To a stirring solution comprised of para-toluenesulfonyl chloride in dichloromethane at 0° C. is introduced excess gaseous dimethylamine. The precipitate is removed by filtration and the filtrate is concentrated in vacuo to obtain the product.

WORKUP

后处理

  1. customThe precipitate is removed by filtration
  2. concentrationthe filtrate is concentrated in vacuo
  3. customto obtain the product