HRID353057
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The compound 4-methyl-3-nitro-benzene-N,N-dimethylsulfonamide is dissolved in ethanol. A catalyst like Raney nickel is added and the mixture hydrogenated in a shaker. The catalyst is removed by filtration. The solvent is removed in vacuo to give a product which may be purified if necessary by chromatography or crystallization from an appropriate solvent like chloroform or heptane-ethyl acetate.
WORKUP
后处理
- customThe catalyst is removed by filtration
- customThe solvent is removed in vacuo
- customto give a product which
- custommay be purified if
- customnecessary by chromatography or crystallization from an appropriate solvent like chloroform or heptane-ethyl acetate