HRID353057

反应详情

EQUATION

反应方程式

HRID 353057 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The compound 4-methyl-3-nitro-benzene-N,N-dimethylsulfonamide is dissolved in ethanol. A catalyst like Raney nickel is added and the mixture hydrogenated in a shaker. The catalyst is removed by filtration. The solvent is removed in vacuo to give a product which may be purified if necessary by chromatography or crystallization from an appropriate solvent like chloroform or heptane-ethyl acetate.

WORKUP

后处理

  1. customThe catalyst is removed by filtration
  2. customThe solvent is removed in vacuo
  3. customto give a product which
  4. custommay be purified if
  5. customnecessary by chromatography or crystallization from an appropriate solvent like chloroform or heptane-ethyl acetate