HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178486092, compound → HCID 178486091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178486092 | HCID 178486092 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178486091 | HCID 178486091 | — |
Reaction Steps
The compound 4-methyl-3-nitro-benzene-N,N-dimethylsulfonamide is dissolved in ethanol. A catalyst like Raney nickel is added and the mixture hydrogenated in a shaker. The catalyst is removed by filtration. The solvent is removed in vacuo to give a product which may be purified if necessary by chromatography or crystallization from an appropriate solvent like chloroform or heptane-ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06750217B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-c3f4191d7f0a491baafd4427f8094f1c |
| Source note | uspto-grants-2004_06 |