HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86587979, compound → HCID 22707298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86587979 | HCID 86587979 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22707298 | HCID 22707298 | — |
Reaction Steps
The compound 2-(2-chloro-4-iodo-phenylamino)-4-dimethylsulfamoyl-benzoic acid O-(tetrahydro-2H-pyran-2-yl)-oxyamide is dissolved in an appropriate hydrogen chloride-saturated solvent like methanol or ethanol. Once homogeneous, the solution is concentrated in vacuo to give the desired product. The product may be triturated with an appropriate solvent like chloroform or dichloromethane if further purification is necessary.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06750217B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-cb0830ebcaa84aad91c48e3968a060eb |
| Source note | uspto-grants-2004_06 |