HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Phthalylglycine aldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | N-(2-Hydroxyethyl)phthalimide | HCID 77499 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Phthalylglycine aldehyde | HCID 76201 | 74% |
Reaction Steps
The preparation from N-(2-hydroxyethyl)phthalimide was carried out as in example 2; cooling was carried out by means of tap water. Yield: 74%, m.p. 114° C. (from methylene chloride).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06750371B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-21e785f0d9014f708923c2354e9fed55 |
| Source note | uspto-grants-2004_06 |