HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 23513849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Product | HCID 23513849 | HCID 23513849 | — |
Reaction Steps
4-{[Bis-(2-hydroxyethyl)-amino]-methyl}benzonitrile was prepared according to the general method as outlined in Example 1 (Step 4) starting from diethanolamine (10.2 g, 97 mmol) and α-bromo-p-tolunitrile (15.8 g, 81 mmol). Yield, (68%); white solid; mp 163° C. MS: 221.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06753337B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-877c7931cd1943078bac2094a3ad81fc |
| Source note | uspto-grants-2004_06 |