HRID353629

反应详情

EQUATION

反应方程式

HRID 353629 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Pearlman's catalyst (20% w/w palladium hydroxide-on-carbon) (1.5 g) was added to a solution of cyclopentylamine (15 ml, 0.21 mol) in acetone (200 ml). The reaction mixture was stirred under an atmosphere of hydrogen gas at 414 kPa (60 psi). After stirring for 16 hours the reaction mixture was filtered through Arbocel (trade mark) and the solvent removed under reduced pressure to give the title compound (15 ml) as a thin oil.

WORKUP

后处理

  1. stirringAfter stirring for 16 hours the reaction mixture
  2. filtrationwas filtered through Arbocel (trade mark)
  3. customthe solvent removed under reduced pressure