HuagongsheHuagongshe Chemistry Print Report · For research reference only
DL-Carnitine → Cyclohexyl acetyl carnitine chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | DL-Carnitine | HCID 288 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Cyclohexylacetyl chloride | HCID 2757989 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | Cyclohexyl acetyl carnitine chloride | HCID 131715698 | — |
Reaction Steps
Carnitine chloride (2.97 g; 0.01 moles) was dissolved in trifluoro acetic acid (10 cc). To this solution was added cyclohexyl acetyl chloride (0.01 moles) prepared as previously disclosed and the resulting mixture was kept under stirring for 48 hours. Ethyl ether was then added and the resulting mixture was kept under stirring for 0.5 hours at 0° C. A precipitate was obtained, which was filtered off and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766222 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-ccb56ca24b4b4916a6432cb595293d2a |
| Source note | uspto-grants-1988_08 |