HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → 2-Acetamidomethyl-6-chlorosulfonyl-4-(1,1-dimethylethyl)-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | N-[(5-tert-Butyl-2-hydroxyphenyl)methyl]acetamide | HCID 13210348 | — |
| Product | 2-Acetamidomethyl-6-chlorosulfonyl-4-(1,1-dimethylethyl)-phenol | HCID 13210349 | — |
Reaction Steps
15.5 g (0.059 mole) of 2-acetamidomethyl-4-(1,1-dimethylethyl)-phenol are introduced at room temperature into 100 ml of chlorosulfonic acid. Stirring is continued for a further 15 minutes and the solution is stirred into ice water. The precipitate is filtered off with suction and recrystallized from toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766241 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-3b69f045a12647a1bf61c0c7bf75b4dc |
| Source note | uspto-grants-1988_08 |