Potassium Carbonate → HCID 13104837, compound

Participants

Reaction Steps

1-[[2-(2-(4-Chlorophenyl)ethyl)-4-(2-chlorophenoxymethyl)-1,3-dioxolan-2-yl]methyl]imidazole nitrate (2.0 g) in 100 ml of dichloromethane was shaken with excess dilute potassium carbonate solution until the salt was completely dissolved. The organic layer was then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[[2-(2-(4-chlorophenyl)ethyl)-4-(2-chlorophenoxymethyl)-1,3-dioxolan-2-yl]methyl]imidazole as an oil.

Provenance & Evidence