HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → N-Cyclohexyl-N'-phenylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | N-Cyclohexyl-N'-phenylurea | HCID 13451 | — |
Reaction Steps
5.26 g (0.02 mole) of(2-methyl 1-phenyloxy 2-hydroxy propyl)-cyclohexylamine is dissolved in 300 ml of benzene. 2.38 g (0.02 mole) of phenylisocyanate were added. Slight heating was observed as well as the appearance of a solid. It was heated under reflux for 1 hour. After cooling, it was filtered and the product was recrystallized in ethanol. Melting point 164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04376783 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-1e01f692b3ff47e184ea12f2104473ac |
| Source note | uspto-grants-1983_03 |