alpha-Fluoro-3-phenoxybenzylbromide → alpha-Fluoro-3-phenoxybenzyl alpha-isopropyl-(3,4-dichlorophenyl)acetate

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Reaction Steps

This compound was prepared from α-isopropyl-(3,4-dichlorophenyl)acetic acid and α-fluoro-3-phenoxybenzylbromide following the procedure described in Example 2 Method B. The product, a colourless oil, was characterised by pmr spectroscopy. Chemical shift δppm (solvent CDCl3): 0.76 (3H, d, J=6 Hz, CH3); 1.07 (3H, d of d, J=6 Hz and J=2 Hz, CH3); 2.33 (1H, m, --CH(CH3)2); 3.28 (1H, d, J=10 Hz, CH); 7.24 (1H, d of d, J=56 Hz and J=2 Hz, CHF) and about 7.33 (12H, m, aromatic protons).

Provenance & Evidence