HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(o-fluorophenyl)-1,3-dihydro-1,3,3-trimethyl-7-nitro-2H-1,4-benzodiazepin-2-one → 2-Amino-5-nitro-2'-chlorobenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(o-fluorophenyl)-1,3-dihydro-1,3,3-trimethyl-7-nitro-2H-1,4-benzodiazepin-2-one | HCID 20506156 | — |
| Reactant | 2-Amino-2'-(o-chlorobenzoyl)-2-methyl-4'-nitro-propionanilide | HCID 20506169 | — |
| Product | 2-Amino-5-nitro-2'-chlorobenzophenone | HCID 74830 | — |
Reaction Steps
From 70 g (0.25 mol) of 2-amino-5-nitro-2'-chlorobenzophenone there is obtained, in analogy to the details in paragraph (a) of Example 1, 2-amino-2'-(o-chlorobenzoyl)-2-methyl-4'-nitro-propionanilide of melting point 138°-139° (ether/petroleum ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377522 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-28c573fa77904a8f9841e0698735e739 |
| Source note | uspto-grants-1983_03 |