HRID354744

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CN1C(=O)C(C)(C)N=C(c2ccccc2F)c2cc([N+](=O)[O-])ccc21

HCID20506156

未命名化合物

结构：CC1(C)N=C(c2ccccc2Cl)c2cc([N+](=O)[O-])ccc2NC1=O

HCID20506168

5-(o-chlorophenyl)-1,3-dihydro-3,3-dimethyl-7-nitro-2H-1,4-benzodiazepin-2-one

C17H14ClN3O3

PRODUCTS

生成物

结构：CC(C)(N)C(=O)Nc1ccc([N+](=O)[O-])cc1C(=O)c1ccccc1Cl

HCID20506169

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21226440

未命名化合物

PROCEDURE

实验过程

From 76 g (0.21 mol) of 2-amino-2'-(o-chlorobenzoyl)-2-methyl-4'-nitro-propionanilide there is obtained, in analogy to the details in paragraph (b) of Example 1, 5-(o-chlorophenyl)-1,3-dihydro-3,3-dimethyl-7-nitro-2H-1,4-benzodiazepin-2-one of melting point 242° (methylene chloride/n-hexane).