HRID354759

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)N1C(=O)C(C)(C)N=C(c2ccccc2Cl)c2cc(NC(=O)NCCO)ccc21

HCID20506159

未命名化合物

结构：CC(C)N1C(=O)C(C)(C)N=C(c2ccccc2Cl)c2cc(N=C=O)ccc21

HCID20506187

未命名化合物

PRODUCTS

生成物

结构：CC(C)N1C(=O)C(C)(C)N=C(c2ccccc2Cl)c2cc(N)ccc21

HCID20506147

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID22020333

未命名化合物

PROCEDURE

实验过程

From 4 g (0.011 mol) of 7-amino-5-(o-chlorophenyl)-1,3-dihydro-1-isopropyl-3,3-dimethyl-2H-1,4-benzodiazepin-2-one there is obtained, in analogy to the details in Example 4, via [5-(o-chlorophenyl)-2,3-dihydro-1-isopropyl-3,3-dimethyl-2-oxo-1H-1,4-benzodiazepin-7yl]isocyanate, 1-[5-(o-chlorophenyl)2,3-dihydro-1-isopropyl-3,3-dimethyl-2-oxo-1H-1,4-benzodiazepin-7-yl]-3-(2-hydroxyethyl)urea of melting point 243°-244° (1,2-dichloroethane/methylene chloride).