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HRID354772

反应详情

EQUATION

反应方程式

HRID 354772 的结构方程式

REACTANTS

反应物

3
结构：CCCBr
HCID7840

1-Bromopropane

C3H7Br

结构：CN1C(=O)C(C)(C)N=C(c2ccccc2F)c2cc([N+](=O)[O-])ccc21
HCID20506156

未命名化合物

结构：CCCN1C(=O)C(C)(C)N=C(c2ccccc2F)c2cc([N+](=O)[O-])cc(Cl)c21
HCID20506198

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)N=C(c2ccccc2F)c2cc([N+](=O)[O-])cc(Cl)c2NC1=O
HCID20506164

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOCC
溶剂HCID21584099

Diethylether hexane

C10H24O

PROCEDURE

实验过程

From 32 g (0.088 mol) of 9-chloro-5-(o-fluorophenyl)-1,3-dihydro-3,3-dimethyl-7-nitro-2H-1,4-benzodiazepin-2-one and propyl bromide there is obtained, in analogy to the details in paragraph (c) of Example 1, with a reaction period of 3 days, 9-chloro-5-(o-fluorophenyl)-1,3-dihydro-3,3-dimethyl-7-nitro-1-propyl-2H-1,4-benzodiazepin-2-one of melting point 142°-143° (ether/n-hexane).