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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 354821Generated: October 28, 2026

HCID 20506402, compound → HCID 20506389, compound

https://huagongshe.com/reaction/354821

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 20506402HCID 20506402—
ReactantHCID 53720619HCID 53720619—
SolventIsoamyl AlcoholHCID 31260—
ProductHCID 20506389HCID 20506389—

Reaction Steps

A mixture of 0.1 mole of 2-methylmercapto-4-amino-6-chloro-7,8-dimethoxyquinazoline and 0.12 mole of 3-n-hexylpyrrolidine in isoamyl alcohol is heated at reflux for 16 hours, cooled, washed with water and the organic phase is concentrated in vacuo. Hexane is slowly added to the residue and the solid title compound is collected and purified, if desired by silica gel column chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04377581
Source datasetuspto-grants-1983_03
ORD IDord-dea54653d3d243b79e7d6ca9787b9004
Source noteuspto-grants-1983_03