HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20506402, compound → HCID 20506389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20506402 | HCID 20506402 | — |
| Reactant | HCID 53720619 | HCID 53720619 | — |
| Solvent | Isoamyl Alcohol | HCID 31260 | — |
| Product | HCID 20506389 | HCID 20506389 | — |
Reaction Steps
A mixture of 0.1 mole of 2-methylmercapto-4-amino-6-chloro-7,8-dimethoxyquinazoline and 0.12 mole of 3-n-hexylpyrrolidine in isoamyl alcohol is heated at reflux for 16 hours, cooled, washed with water and the organic phase is concentrated in vacuo. Hexane is slowly added to the residue and the solid title compound is collected and purified, if desired by silica gel column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377581 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-dea54653d3d243b79e7d6ca9787b9004 |
| Source note | uspto-grants-1983_03 |