Methoxyacetyl chloride → HCID 13209079, compound

Participants

Reaction Steps

15.2 g of methoxyacetyl chloride are added dropwise at room temperature to 32 g of N-(1'methoxycarbonylethyl)-2,6-dimethyl-3-nitroaniline. After the weakly exothermic reaction has subsided, the reaction solution is stirred for 20 hours at room temperature. The solvent is then removed and the dark red oily residue is distilled in a high vacuum. Compound 28 distills at a temperature of 170°-174° C. and a pressure of 0.07 mbar as a pale yellow oil.

Provenance & Evidence