HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Diethylthiourea → HCID 20506556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Diethylthiourea | HCID 2735009 | — |
| Reactant | 3-Bromo-1,1-diphenylacetone | HCID 2794635 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20506556 | HCID 20506556 | — |
Reaction Steps
To a filtered solution of 1.32 g. of 1,3-diethyl-2-thiourea in 25 ml. of acetone is added a filtered solution of 3-bromo-1,1-diphenyl-2-propanone in 25 ml. of acetone. The mixture is allowed to stand, then the solid is collected by filtration, washed with acetone and dried in vacuo, giving 3.73 g. of the desired product, m.p. 174°-176° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377589 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-2827049d555644459acdb2003933a016 |
| Source note | uspto-grants-1983_03 |