HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15341898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 17beta-Tetrahydropyranyloxy-5alpha-androstan-4-one | HCID 15341897 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15341898 | HCID 15341898 | 116.7% |
Reaction Steps
To 75 ml of ethanol is added 2.32 g of the product of Step E to form a solution which is then treated with 5 ml of 2.5 N hydrochloric acid and warmed on a steam bath for 40 min. to yield 2.1 g of a crystalline product having a m.p. of 123°-126° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377584 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-7add9fb1d282489394e78ccb92ff4e39 |
| Source note | uspto-grants-1983_03 |