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HRID354914

反应详情

EQUATION

反应方程式

HRID 354914 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：C[C@]12CCCC(=O)[C@@H]1CC[C@@H]1[C@@H]2CC[C@]2(C)[C@@H](OC3CCCCO3)CC[C@@H]12
HCID15341897

未命名化合物

PRODUCTS

生成物

1
结构：C[C@]12CCCC(=O)[C@@H]1CC[C@@H]1[C@@H]2CC[C@]2(C)[C@@H](O)CC[C@@H]12
HCID15341898

未命名化合物

收率 116.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

To 75 ml of ethanol is added 2.32 g of the product of Step E to form a solution which is then treated with 5 ml of 2.5 N hydrochloric acid and warmed on a steam bath for 40 min. to yield 2.1 g of a crystalline product having a m.p. of 123°-126° C.

WORKUP

后处理

  1. customto form a solution which
  2. temperaturewarmed on a steam bath for 40 min.