HuagongsheHuagongshe Chemistry Print Report · For research reference only
2(3H)-Benzoxazolone → HCID 12961163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2(3H)-Benzoxazolone | HCID 6043 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 8-bromooctanoate | HCID 264813 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12961163 | HCID 12961163 | — |
Reaction Steps
The product is produced as described in example 1 from 3.0 g. of NaH (80% suspension in mineral oil), 13.5 g. of benzoxazolin-2-one, 200 cc. of DMF, 23.7 g. of 8-bromocaprylic acid ethyl ester and 3.0 g. of NaJ. Eluant in chromatographic purification: hexane/ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377695 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-a613b0c8aa5a4d349fe13179d522a3b6 |
| Source note | uspto-grants-1983_03 |