HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 54164349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Reactant | 8-(2-Oxobenzimidazolin-1-yl)-caprylic acid methyl ester | HCID 12961171 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54164349 | HCID 54164349 | — |
Reaction Steps
The product is produced as described in example 1 from 0.75 g. of NaH (80% suspension in mineral oil), 5.6 g. of 1-benzylbenzimidazolin-2-one (produced in usual manners by alkylation of benzimidazolin-2-one with benzylchloride according to example 8), 50 cc. of DMF, 5.9 g. of 8-bromocaprylic acid methyl ester and 0.75 g. of NaJ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377695 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-fdb769078caf46fbb94c01b9cc831d09 |
| Source note | uspto-grants-1983_03 |