HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → RU 59063
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 22116972 | HCID 22116972 | — |
| Product | RU 59063 | HCID 197655 | — |
Reaction Steps
Using the procedure of Example 71, 300 mg of the product of Example 76 were reacted to obtain 236 mg of the expected product melting at 78°-79° C. with a Rf=0.31 (eluant: methylene chloride--acetone (75-25)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE035956 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-6e101122724b4796b0920631581ec140 |
| Source note | uspto-grants-1998_11 |