Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phthalonitrile | HCID 7042 | — |
| Reactant | HCID 131719385 | HCID 131719385 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | Gallium phthalocyanine | HCID 136138306 | — |
Reaction Steps
A mixture of 29.1 parts of phthalonitrile, 9.2 parts of gallium trimethoxide, and 150 parts of ethylene glycol was stirred for 24 hours at 200° C. in a nitrogen atmosphere, and the product was filtered. The product was successively washed with N,N-dimethylformamide and then methanol, and dried to provide 23.0 parts of gallium phthalocyanine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05834149 |
|---|
| Source dataset | uspto-grants-1998_11 |
|---|
| ORD ID | ord-6a845a6c48a24eedaa0d7c9939fef0a4 |
|---|
| Source note | uspto-grants-1998_11 |
|---|
