HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl vinyl ketone → HCID 21829922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl vinyl ketone | HCID 6570 | — |
| Reactant | HCID 21829902 | HCID 21829902 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21829922 | HCID 21829922 | 97.4% |
Reaction Steps
Methyl vinyl ketone (1.02 g) was added to a solution of N-(2,5-dichlorophenyl)-2-aminoisobutyramide (2.4 g) in tetrahydrofuran (10 mL) and the mixture was heated at reflux for 30 hours. After distilling off the solvent under reduced pressure, 3 g of N-(2,5-dichlorophenyl)-2-(3-oxobutylamino)isobutyramide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834401 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-4b09b83902e44bc7aedaeb57c56f6a99 |
| Source note | uspto-grants-1998_11 |