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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 355783Generated: October 30, 2026

Oxalyl chloride → 4-[2-Benzyloxybenzylthio]benzoylchloride

https://huagongshe.com/reaction/355783

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant4-[2-Benzyloxybenzylthio]benzoic acidHCID 22675551—
SolventDichloromethaneHCID 6344—
Product4-[2-Benzyloxybenzylthio]benzoylchlorideHCID 22675537—

Reaction Steps

4-[2-benzyloxybenzylthio]benzoic acid (6.3 g) and oxalyl chloride (2.26 g) were stirred in dichloromethane (100 ml) for 18 hours. The solvent was evaporated to give 4-[2-benzyloxybenzylthio]benzoylchloride which was dissolved in dichloromethane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05834468
Source datasetuspto-grants-1998_11
ORD IDord-06d9ef70417f4a468e359f0480f5b61d
Source noteuspto-grants-1998_11