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HRID355783

反应详情

EQUATION

反应方程式

HRID 355783 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)C(=O)Cl
HCID65578

Ethanedioyl dichloride

C2Cl2O2

结构：O=C(O)c1ccc(SCc2ccccc2OCc2ccccc2)cc1
HCID22675551

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Cl)c1ccc(SCc2ccccc2OCc2ccccc2)cc1
HCID22675537

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

4-[2-benzyloxybenzylthio]benzoic acid (6.3 g) and oxalyl chloride (2.26 g) were stirred in dichloromethane (100 ml) for 18 hours. The solvent was evaporated to give 4-[2-benzyloxybenzylthio]benzoylchloride which was dissolved in dichloromethane.

WORKUP

后处理

  1. customThe solvent was evaporated