HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 18940716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18940731 | HCID 18940731 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18940716 | HCID 18940716 | 97% |
Reaction Steps
The compound was synthesized by mixing (Compound 8) (0.6 g, 1.9 mmol), 1-bromo-3-chloropropane (0.45 g, 2.9 mmol), NaH (0.09 g, 2.3 mmol) in DMF, in the same manner as illustrated in example 3 to give the title compound (0.72 g, 97%). M.p. 192°-195° C. (and 235.5°-236° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834482 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-fba097e91d5d4cc095bb706d2ed14a85 |
| Source note | uspto-grants-1998_11 |