HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenylpiperidin-4-ol → HCID 18940711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenylpiperidin-4-ol | HCID 96387 | — |
| Reactant | HCID 18940716 | HCID 18940716 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18940711 | HCID 18940711 | 43% |
Reaction Steps
The compound was synthesized by mixing (Compound 9) (0.7 g, 1.8 mmol), 4-phenylpiperidin-4-ol (0.38 g, 2.2 mmol) and TEA (0.55 g, 5.4 mmol) in DMF, in the same manner as illustrated in example 4 to give the title compound (0.47 g, 43%). M.p. 184°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834482 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-d5dee6dd149d46a6ac22667727482768 |
| Source note | uspto-grants-1998_11 |