HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 18940712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 53671852 | HCID 53671852 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18940712 | HCID 18940712 | 7% |
Reaction Steps
The compound was synthesized by mixing (Compound 12) (3.0 g, 8.8 mM), NaH (0.46 g, 11.0 mmol) and 1-bromo-3-chloropropane (1.5 g, 9.7 mmol) in DMF, in the same manner as illustrated in example 3 to give the title compound (0.25 g, 7%). M.p. 223°-224° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834482 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-44494bba29e84f8782df9b1b1013e6fa |
| Source note | uspto-grants-1998_11 |