HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 6-nitro-9H-beta-carboline-3-carboxylate → HCID 603089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 6-nitro-9H-beta-carboline-3-carboxylate | HCID 13037332 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 603089 | HCID 603089 | 79% |
Reaction Steps
A suspension of Pd (10% on carbon, 1.0 g), and Compound 15 (8.0 g, 28 mmol) in anhydrous ethanol (300 mL) was hydrogenated (2280 mL) at 1 atm. The reaction mixture was filtered through a filter aid. The filtrate was concentrated in vacuo to give the title compound (5.62 g, 79%). M.p. 226°-228° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834482 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-08d03a02c79b4aae8ea03540d63662db |
| Source note | uspto-grants-1998_11 |