HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 54296990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 54192254 | HCID 54192254 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54296990 | HCID 54296990 | 28% |
Reaction Steps
The compound was synthesized by mixing (Compound 18) (1 g, 2.8 mmol), NaH (50% in oil) (0.075 g, 3.1 mmol) and 1-bromo-3-chloropropane (0.44 g, 3.1 mmol) in DMF in the same manner as illustrated in example 3 to give the title compound (0.35 g, 28%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834482 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-9fdf7782145446e8bea53468c8e25e1b |
| Source note | uspto-grants-1998_11 |