HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Chloromethyl)pyridine → HCID 18940845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Chloromethyl)pyridine | HCID 18358 | — |
| Reactant | HCID 178488093 | HCID 178488093 | — |
| Product | HCID 18940845 | HCID 18940845 | — |
Reaction Steps
The above mentioned compound was prepared analogously to the procedure described in J. Het. Chem. 3, 67 (1966) from 5-methoxy-indolyl-magnesium bromide and 3-chloromethylpyridine. After purification by Flash Chromatography on silica gel using as eluent methylene chloride/methanol/ammonia (98:2:0,1), the desired compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834493 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-7cd41f2ba4a44347be66caba0f7dd3a8 |
| Source note | uspto-grants-1998_11 |