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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 355986Generated: October 29, 2026

Benzyl Bromide → HCID 18940826, compound

https://huagongshe.com/reaction/355986

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl BromideHCID 7498—
ReactantHCID 18940845HCID 18940845—
SolventMethyl Ethyl KetoneHCID 6569—
ProductHCID 18940826HCID 18940826—

Reaction Steps

Benzyl bromide (8.7 ml; 0.073 mol) was added to a stirring mixture of compound of Description 1 [5-methoxy-3-(pyridin-3-ylmethyl)-1H-indole] (3.5 g; 0.0146 mol) in methyl ethyl ketone (70 ml). The reaction mixture was refluxed for 3 hours. The product precipitated as a yellow solid was filtered and washed with diethyl ether and dried under vacuum. The compound was used as such without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05834493
Source datasetuspto-grants-1998_11
ORD IDord-99013408221a4cf28fd386bd06d49186
Source noteuspto-grants-1998_11