HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 18940826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 18940845 | HCID 18940845 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 18940826 | HCID 18940826 | — |
Reaction Steps
Benzyl bromide (8.7 ml; 0.073 mol) was added to a stirring mixture of compound of Description 1 [5-methoxy-3-(pyridin-3-ylmethyl)-1H-indole] (3.5 g; 0.0146 mol) in methyl ethyl ketone (70 ml). The reaction mixture was refluxed for 3 hours. The product precipitated as a yellow solid was filtered and washed with diethyl ether and dried under vacuum. The compound was used as such without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834493 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-99013408221a4cf28fd386bd06d49186 |
| Source note | uspto-grants-1998_11 |