Hydrochloric Acid → HCID 18940844, compound

HRID 355989Notes

Reaction equation

HRID 355989 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH:7]=[C:6]2[CH2:12][C:13]1[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=1.[ClH:19]>C(OCC)C>[ClH:19].[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH:7]=[C:6]2[CH2:12][C:13]1[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18940845HCID 18940845, compound

Product 1

HCID 18940844HCID 18940844, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A solution of compound of Description 1 [5-methoxy-3-(pyridin-3-ylmethyl)-1H-indole] (3 g) in diethyl ether was saturated with gaseous hydrogen chloride. A solid was precipitated. The title compound was collected by filtration washed with diethyl ether and dried under vacuum. The compound was used as such without further purification.

Workup

  1. customA solid was precipitated
  2. filtrationThe title compound was collected by filtration
  3. washwashed with diethyl ether
  4. customdried under vacuum
  5. customsuch without further purification

Sources & evidence

ORD record
ord-bad3ff91bc624a9690413883c538b5c1
Source dataset
uspto-grants-1998_11
Patent number
US05834493

Reaction notes

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