Methyl iodide → HCID 18940820, compound

Participants

Reaction Steps

Methyl iodide (10.4 ml; 0.167 mol) was added to a stirring mixture of compound of Description 1 [5-methoxy-3-(pyridin-3-ylmethyl)-1H-indole] (5.3 g; 0.022 mol) in acetone (150 ml). The reaction mixture was stirred at room temperature for 18 hours. The reaction mixture was concentrated under vacuum. The residual solid was washed with diethyl ether giving the desired compound (7.5 g).

Provenance & Evidence