HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 10708316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 18940938 | HCID 18940938 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 10708316 | HCID 10708316 | 92.1% |
Reaction Steps
The thiol (D79) (0.35 g, 1.29 mmol) was treated with K2CO3 (0.20 g, 1.45 mmol) and iodomethane (0.24 ml, 3.85 mmol) in DMSO (15 ml) at 50° C. as in the method of Description 80 to afford the title compound (0.34 g, 92%) as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-5a13965fc6b64fd0ba70358fb0b19973 |
| Source note | uspto-grants-1998_11 |