HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatopyridine → HCID 10710785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatopyridine | HCID 2760493 | — |
| Reactant | HCID 18940897 | HCID 18940897 | — |
| Product | HCID 10710785 | HCID 10710785 | 84% |
Reaction Steps
4-Chloro-5-methylthioindoline (D49) (0.9 g, 4.51 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The crude product was filtered-off and recrystallised from ethanol to give the title compound (1.22 g, 84%) as a white crystalline solid m.p. 237°-241° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-ba4d324284f4471aa6fb3c776d733e43 |
| Source note | uspto-grants-1998_11 |