HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatopyridine → HCID 10518435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatopyridine | HCID 2760493 | — |
| Reactant | HCID 18940898 | HCID 18940898 | — |
| Product | HCID 10518435 | HCID 10518435 | 59% |
Reaction Steps
6-Chloro-5-ethylindoline (D52) (0.42 g, 2.33 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The crude product was recrystallised from ethanol/diethyl ether to give the title compound (0.42 g, 59%) as a white crystalline solid m.p.=227° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-f2175825a4f24d35bca6823bd4dca5b3 |
| Source note | uspto-grants-1998_11 |