HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatopyridine → HCID 10687827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatopyridine | HCID 2760493 | — |
| Reactant | HCID 10632224 | HCID 10632224 | — |
| Product | HCID 10687827 | HCID 10687827 | 58% |
Reaction Steps
4-Chloro-5-tert-butylindoline (D57) (0.45 g, 3.04 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The product was recrystallised from ethanol/diethyl ether to give the title compound (0.46 g, 58%) as a white crystalline solid m.p.=174°-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-cd6e00dc51fb4a0c96c36f4b9e1c1cf1 |
| Source note | uspto-grants-1998_11 |