HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatopyridine → HCID 18940921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatopyridine | HCID 2760493 | — |
| Reactant | HCID 18940936 | HCID 18940936 | — |
| Product | HCID 18940921 | HCID 18940921 | 61% |
Reaction Steps
6-Chloro-5-isopropylthioindoline (D66) (0.35 g, 1.52 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The crude product was recrystallised from ethanol/diethyl ether to give the title compound (0.33 g, 61%) as a white crystalline solid m.p. 199°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-e16d98046cf7445d801316ec65781179 |
| Source note | uspto-grants-1998_11 |