HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatopyridine → HCID 9976912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatopyridine | HCID 2760493 | — |
| Reactant | HCID 18940893 | HCID 18940893 | — |
| Product | HCID 9976912 | HCID 9976912 | 70% |
Reaction Steps
6-Bromo-5-ethylthioindoline (D84) (0.28 g, 1.09 mmol) was treated with 3-pyridylisocyanate as in the procedure described in Example 1. The product was recrystallised from ethanol/diethyl ether to yield the title compound (0.29 g, 70%) as an off-white crystalline solid m.p. 226°-227° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834494 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-fe3c2d5b17f14000bbbc3a6dc1742be4 |
| Source note | uspto-grants-1998_11 |