HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 18941023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 18941027 | HCID 18941027 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18941023 | HCID 18941023 | — |
Reaction Steps
In 42 ml of 29% aqueous ammonia and 60 ml of methanol, 1.48 g of 6-tert-butoxycarbonyl-6-azabicyclo[3.2.0]heptane-7-thione was dissolved, followed by stirring at room temperature for 30 minutes. The solvent was azeotropically evaporated using benzene-ethanol, whereby 1.39 g of 2-(tert-butoxycarbonylamino)cyclopentanecarbothioamide was obtained as the crystal form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834499 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-d84fb4f9c0dc4d93b1a527826df6d64c |
| Source note | uspto-grants-1998_11 |