HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 70111952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 70111953 | HCID 70111953 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70111952 | HCID 70111952 | — |
Reaction Steps
In ethanol was dissolved (3aR*,10aS*)-9-benzyl-1,2,3,3a,4,9,10,10a-octahydrobenzo[b]cyclopenta-[e][1,4]diazepine produced in Working Example 42. To the solution was added a 2.43N HCl-ethanol solution. This solution was concentrated under reduced pressure, and the concentrate was crystallized from ethanol to give the titled compound, m.p. 177°-179° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834463 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-abc4baa8168c48a48972e7c78ba9af1c |
| Source note | uspto-grants-1998_11 |